Duff Sample Clauses

Duff. Dec a y i n g pl a n t m a tt e r t h a t i n- cl u des le xx xx tt e r , g r ee n w a s t e, s t e m m a t e r i a l , b a r k , a n d a ny o t h e r pl a n t m a t e r i a l t h a t , u po n vis u a l i n spec t io n , does n o t a ppe a r t o h a ve co m ple t el y de- co m posed i n t o soil.
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Duff. Samples of duff material will be collected, handled, and documented in general accordance with Site-specific SOP EPA-XXXXX-2012-11, Sampling and Analysis of Duff for Asbestos (see Appendix B), with the following project modifications: ▪ Duff material will be collected in close proximity to the three trees selected for tree bark sampling. ▪ Enough material will be collected from each sub-location such that the material from the three sub-locations fills a 1-gallon zip-top bag. ▪ Sample information will be recorded on a soil FSDS (the soil FSDS is designed to accommodate multiple media). In brief, at each specified sampling point, any fresh or partially decayed organic debris (e.g., twigs, leaves, pine needles) will be collected by hand from the soil surface, taking care to ensure that the top layer of soil beneath the organic debris is not included in the duff material sample.
Duff. Sample Preparation Duff samples will be prepared and analyzed in basic accordance with the procedures specified in SOP EPA-XXXXX-2012-11, Sampling and Analysis of Duff for Asbestos (see Appendix B). In brief, each sample is dried and ashed, and an aliquot of the resulting ash residue is acidified, suspended in water, and filtered. The resulting filter will be used to prepare a minimum of three grids using the grid preparation techniques described in Section 9.3 of ISO 10312:1995(E). Any remaining ash material will be archived for possible future analysis. For 10% of the duff samples, two additional ash aliquots will be prepared to filters and analyzed to gain an understanding of the within-sample variability. These samples will be selected post hoc (i.e., after the results have been received for the field samples) by the FTL (or their designee) so that a range of duff concentrations are represented. Analysis Method and Counting Rules Grids will be examined by TEM using high magnification (~20,000x) in basic accordance with the recording procedures described in ISO 10312:1995(E), as modified by SOP EPA-XXXXX-2012- 11 and the most recent versions of Xxxxx Laboratory Modifications3 LB-000016, LB-000029, LB- 000066, LB-000067, and LB-000085. In brief, all fibrous amphibole structures that have appropriate SAED patterns and EDXA spectra, and having length ≥ 0.5 um and an aspect ratio (length: width) ≥ 3:1, will be recorded. If observed, chrysotile structures should be recorded using the same procedures. Stopping Rules The stopping rules for the TEM analysis of duff materials are as follows:

Related to Duff

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