Collect Samples of VOC and Methane Using SUMMA Canisters Sample Clauses

Collect Samples of VOC and Methane Using SUMMA Canisters. The objective of this sub-task is to determine compound-specific emission rates by collecting VOC and methane samples using SUMMA canisters. Although ideal, it is not economically feasible to collect this data at each site. Therefore, collection of these samples will be taken at a representative number of point sources, which then can be used as surrogates for the entire population. An example of a SUMMA canister is presented below. The canister samples will be collected at the exhaust port of the HiFlow Sampler and sent to TestAmerica laboratories in Austin, Texas for general hydrocarbon analyses (Analytical Method TO-15), and for methane analyses (Analytical Method D-1946). Information about these two analytical methods is provided in Appendix A. Because emission rate data from the HiFlow Sampler is basically expressed as % total hydrocarbon per cubic foot/minute (i.e., methane response factors), we will be able to use the results of the Summa canister analysis to determine the emission rate for individual compounds, such as benzene, toluene, methane, ethane, propane, butane, etc. For typical sampling scenarios, it is expected that no more than one canister sample will need be collected to characterize multiple IR-detected emissions at any one facility. The reason is that once the emission rate as methane has been measured with the HiFlow Sampler, the same constituent proportions identified in a single canister sample can be assumed for all emission sources at that same facility. In other words, if three IR-detected emissions are identified at the same facility, the emission rate for each will be determined with the HiFlow Sampler but only one canister sample will be collected and used to calculate speciated emission rates for all three. Atypical sampling scenarios occur if the speciation profile of additional sources is expected to be different from the majority of sources. For example, sites with saltwater tanks may have a toxics speciation profile that is different, thus requiring multiple canister sampling. Speciated emission rates will be reported in pounds per hour, unless other units are requested. The following information will be collected when VOC and methane samples are collected: • Canister ID#; • Canister Sample Number; • Canister Initial Vacuum (inch-Hg); • Canister Sample Start Time (HH:MM:SEC); • Canister Sample Stop Time (HH:MM:SEC); and • Canister Final Vaccuum (inch-Hg). In addition to the canisters that will be sent for laboratory ana...
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