Calculated effects of main operation parameters on Ru Sample Clauses

Calculated effects of main operation parameters on Ru. Pt ratio At the outlet, all eight ratios were used to calculate the effect of the experimental conditions. The effects are summarised in Table 19. At the outlet, a large effect of RH is found. RH appears to be confounded by T and RH: both two-way interaction effects are larger than the main effect of RH. The main effect of T and j at the outlet appear to be small. It is plausible that RH is connected to Ru loss through the solubility in water. The negative effect of temperature could be explained by increased solubility with temperature. The same effect was also found when using number of starvation cycles as response factor (Figure 19). The Ru:Pt ratio determination at the anode inlet region was incomplete, as one measurement was lacking. By inserting an average value of the Ru:Pt ratios measured for the missing figure, effects could be calculated. The result is shown in Table 20. Table 19. Calculated effects from Ru:Pt ratio at outlet. Columns 3-5 (titled 1-3) are intermediate calculations used by the Xxxxx' algorithm. Factor Ru/Pt outlet 1 2 3 Effects Mean 0.39 0.73 1.32 2.63 0.329 T 0.34 0.59 1.31 0.04 0.009 RH 0.26 0.63 0.02 -0.09 -0.023 T*RH 0.34 0.68 0.02 -0.10 -0.025 j 0.26 -0.06 -0.13 -0.01 -0.003 T*j 0.38 0.08 0.04 -0.01 -0.002 RH*j 0.39 0.12 0.13 0.18 0.044 X*XX*x 0.00 -0.00 -0.00 -0.00 -0.000 Table 20. Calculated effects from Ru:Pt ratio at inlet. Columns 3-5 (titled 1-3) are intermediate calculations used by the Xxxxx' algorithm. * Average value inserted to be able to calculate effects. Factor Ru/Pt inlet 1 2 3 Effects Mean 0.696 1 3 7 0.833 T 0.476 2 4 0 -0.093 RH 0.761 2 0 1 0.149 T*RH 0.833* 2 0 0 0.106 j 1.020 0 0 1 0.283 X*x 0.000 0 0 0 -0.000 XX*x 1.040 0 0 0 -0.062 T*RH*j 0.995 0 0 0 -0.039 The main effect of current density is shown to be dominating. It was verified by testing both a large and small ratio for the missing test 4 that the effect of j was still the largest effect. Temperature appears to have a negative, whereas the RH has a positive effect on the Ru:Pt ratio. This is congruent with the results from the ex-situ characterisation of the used MEAs as discussed in Section 4.6.5. The benefit of carrying out the statistical analysis shown above is that the interaction between T and RH is quantified. These aspects will be further investigated and reported in a planned publication. The negative effect of j and RH is not clearly understood. By plotting the cell voltage excursions (Figure 23) upon starvation, there is a significant ...
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