Palladium charcoal (5%) until the reaction was complete. The catalyst and solvent were removed and the residue was crystallised from ethanol-diethyl ether (1:1 v/v) to give 4.7 g. 6-(4- aminobenzoylamino)-hexanoic acid; m.p. 132 - 134 degrees C.
Palladium charcoal (5%) until the absorption of hydrogen had ceased. The catalyst was filtered off and the filtrate evaporated to dryness. The residue was taken up in 5 ml. 2N hydrochloric acid, cooled to -5 degrees C. and treated with 2.5 ml. of 10% aqueous sodium nitrite solution. After standing for 30 minutes, the clear solution was added at -5 degrees C. to a solution of 0.5 g. salicylic acid in 20 ml. of a 1N aqueous sodium hydroxide solution. After subsequently standing for 3 hours at 20 degrees C., the reaction mixture was acidified and extracted with diethyl ether to remove unreacted salicylic acid. The aqueous phase was adjusted to pH 7 by adding 1N aqueous sodium hydroxide solution and the resulting solution was evaporated to dryness. The residue was further dried by adding toluene and subsequently evaporating it and the residue then extracted with methanol. The methanolic solution was concentrated to a small volume. After adding diethyl ether and cooling, the disodium salt of 5-(4-(a- dimethylaminocarboxypentylcarbamoyl)-phenylazo]-salicylic acid separated out; m.p. (greater than) 210 degrees C. (decomp.).
Palladium charcoal (5%) until the reaction was complete. The catalyst and solvent were removed to give 5 g. N,N-diethyl-N'-(4-aminobenzoyl)-ethylenediamine in the form of an oil.
Palladium. During each of the Contract Years from and including 2001 through and including 2003, SMC will sell and deliver and Ford will purchase on a monthly basis [***] of Actual
Palladium. During the Contract Year 1999, SMC will sell and --------- deliver and GM will purchase on a monthly basis [***] of Actual Monthly Production. During the Contract Years 2000, 2001, 2002 and 2003, SMC will sell and deliver and GM will purchase on a monthly basis [***] of Actual Monthly Production. The parties acknowledge that the Actual Monthly Production will vary from time to time. If, during the years 1999 through and including 2003, SMC fails to deliver to GM at least [***] Ounces of Palladium pursuant to this Agreement, then the term of this Agreement shall automatically be extended until such time as SMC has delivered to GM, at a rate of [***] of Actual Monthly Production, an aggregate of [***] Ounces of Palladium pursuant to the provisions of this Agreement.
Palladium. The price per Ounce to be paid to SMC by GM for the --------- actual quantities of Palladium delivered pursuant to Section 3 above shall be based on the [***]
Palladium. During each Contract Year, the price to be paid to SMC by Ford for the actual quantities of Palladium delivered pursuant to Section 3 above shall be based on the [ *** ] for the Pricing Month less a discount per Ounce as set forth in the table below opposite such Contract Year. [***] Contract Minimum Ceiling Year Price Price Discount -------- ------- ------- -------- 2001 [***] [***] [***] 2002 [***] [***] [***] 2003 [***] [***] [***] 2004 [***] [***] [***] 2005 [***] [***] [***] 2006 [***] [***] [***] 2007 [***] [***] [***] 2008 [***] [***] [***] 2009 [***] [***] [***] 2010 [***] [***] [***]
Palladium. During each Contract Year, the price to be paid to SMC by Ford for the actual quantities of Palladium delivered pursuant to Section 3 above shall be based on the [***] for the Pricing Month less a discount per Ounce as set forth in the appropriate table below opposite such Contract Year. [***]: For [***]: Contract Minimum Ceiling Year Price Price Discount ---- ----- ----- -------- 2001 [***] [***] [***] 2002 [***] [***] [***] 2003 [***] [***] [***] 2004 [***] [***] [***] 2005 [***] [***] [***] 2006 [***] [***] [***] 2007 [***] [***] [***] 2008 [***] [***] [***] 2009 [***] [***] [***] 2010 [***] [***] [***] For [***]: Contract Minimum Ceiling Year Price Price Discount ---- ----- ----- -------- 2001 [***] [***] [***] 2002 [***] [***] [***] 2003 [***] [***] [***] 2004 [***] [***] [***] 2005 [***] [***] [***] 2006 [***] [***] [***] 2007 [***] [***] [***] 2008 [***] [***] [***] 2009 [***] [***] [***] 2010 [***] [***] [***]
Palladium. Ford will purchase Ounces of Palladium on a monthly basis for each of the 12 months during the term.
Palladium. The London AM Fix Monthly Average for Palladium for the Pricing Month per Ounce if the London AM Fix Monthly Average for Palladium is less than per Ounce or (ii) per Ounce if the London AM Fix Monthly Average for Palladium is greater than or equal to per Ounce.