Field QC Samples Sample Clauses

Field QC Samples. 36 B5.2 Analytical Laboratory 38 B5.2.1 Training/Certifications 38 B5.2.2 Modification Documentation 39
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Field QC Samples. Field QC samples are collected to help ensure that field samples are not contaminated from exogenous sources during sample collection, and to help evaluate the precision of field sample analytical results. Field QC samples are assigned unique field identifiers and are submitted to the analytical laboratory along with the associated field samples. Duff Only one type of field QC sample will be collected as part of the duff sampling portion of this program – field duplicates. Field blanks for duff are not required for this sampling program. Field duplicate samples of duff material will be collected as part of this sampling program at a rate of 5%. The duff field duplicate should be collected at the same approximate locations as the duff sampling points as the parent sample (i.e., within 12 inches of the parent sampling points). It is the responsibility of the FTL to ensure that the field duplicate is collected. The field duplicate is given a unique sample number, and field personnel will record the sample number of the associated co-located sample in the parent sample number field of the FSDS. The same station location is assigned to the field duplicate sample as the parent field sample. Field duplicates will be sent for analysis by the same method as field samples and are blind to the laboratories (i.e., the laboratory cannot distinguish between field samples and field duplicates). Field duplicate results will be compared to the original parent field sample using the Poisson ratio test using a 90% confidence interval (CI) (Xxxxxx 1982). Because field duplicate samples are expected to have inherent variability that is random and may be either small or large, typically, there is no quantitative requirement for the agreement of field duplicates. Rather, results are used to determine the magnitude of this variability to evaluate data usability. Tree Bark Two types of field QC samples may be collected as part of the tree bark sampling portion of this program – equipment rinsates and field duplicates. Field blanks for tree bark are not required for this sampling program. Equipment Rinsates Equipment rinsates are collected to evaluate potential contamination that arises to due inadequate decontamination of sampling equipment. Equipment rinsates will only be collected if non-dedicated field sampling equipment (i.e., hole saws, chisels) are utilized. Following decontamination efforts, the decontaminated equipment (i.e., hole saw, chisel) should be rinsed with clean w...

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