Preparation of tracer solution Sample Clauses

Preparation of tracer solution. The PFCs have limited solubility in water and it is of high importance to prepare a stable and representative tracer solution prior to the experiments. It was thus decided to dissolve the tracer candidates in a solvent with substantially higher PFC solubility than water. Isobutanol was selected as a solvent for the PFCs. A mixture of the selected PFCs was mixed into a sealed vial completely filled with isobutanol. The solution was mixed overnight and samples from the solution were taken at different time intervals to investigate the stability of the solubility of PFCs in the selected solvent. Results are given in Figure 11. This figure gives an overlay of chromatograms for two analysed samples from the tracer solution in isobutanol. The blue chromatogram is an analysis of a sample taken from the solution at day 1 after preparation while the red chromatogram is an analysis of a sample taken from the solution at day 2 after preparation of the solution. As the figure illustrates there is no change in tracer signal over time and therefore the tracer solution is stable and ready to be included in the experiments. In the dynamic experiments HTO was included as a reference tracer. HTO is an ideal water tracer and the tracer response curve for the PFCs will be compared with the tracer response curve of HTO in the experiments. ECD2 B, Back Signal (GEOTERMI\20160617\20160617 2016-06-17 14-00-32\002F0201.D) ECD2 B, Back Signal (GEOTERMI\20160617\20160617 2016-06-17 14-00-32\001F0101.D) Hz 500000 400000 300000 200000 100000 0 3.5
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