IF NITROGEN AND SULFUR ARE ABSENT Sample Clauses

IF NITROGEN AND SULFUR ARE ABSENT. Acidify a portion of the filtrate with dilute nitric acid and add an excess of 5% silver nitrate solution. Precipitation indicates the presence of chloride, bromide or iodide. Silver chloride precipitate is white, silver bromide precipitate is pale yellow and silver iodide precipitate is yellow. Silver chloride, silver bromide and silver iodide have different solubilities in 5% ammonium hydroxide solution. Decant the solvent and treat the precipitate with dilute aqueous ammonia solution. Add 2 mL 5% ammonium hydroxide to the precipitate. Silver chloride is soluble in ammonium hydroxide, silver bromide is slightly soluble and silver iodide is insoluble in ammonium hydroxide solution. The presence of iodine and bromine may be further confirmed by the following tests. These tests may also be used if it is suspected that more than one halogen is present in the compound.
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